Sep 01, 2014 For these experiments, we used a QM-DK low temperature planetary ball-mill (Nanda, Nanjing, China) equipped with an insulation cover and an air cooling machine that used R22 as a cryogen. The weight ratio of starch to balls (Φ10 mm:Φ20 mm = 2:1) in the ceramic (500 mL) and stainless steel pots (500 mL) were 15:1 and 20:1 (w:w), respectively.
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